Solomon Organik Kimya Cozumleri
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Solomon Organik Kimya Cozumleri
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Organik Kimya Soru Çözümleri.This invention relates to a method for producing an aromatic polyester from a bisaryloxybenzaldehyde or a substituted bisaryloxybenzaldehyde as a starting material.
In recent years, various methods for producing aromatic polyesters, including a continuous mass polymerization and solid phase polymerization, have been investigated.
For example, a continuous mass polymerization method is disclosed in Japanese Unexamined Patent Publication (Kokai) No. 47453/1978 and European Patent Publication (Kokai) No. 227034. This method is conducted by dissolving an aromatic dicarboxylic acid in an organic solvent to form an aromatic dicarboxylic acid ester, condensing the ester with an aromatic bis- or tricarboxylic acid ester and subsequently polymerizing the condensate in an aqueous medium.
In these methods, the presence of a catalytic amount of an acid is essential in the polymerization reaction. The reaction, however, can not be conducted by a neutralization of the acid with a base, since a neutralization of the acid with a base disturbs the polymerization reaction.
Further, in the above methods, since a film and a sheet are formed by the polymerization using a vented extruder and a flat die, it is impossible to obtain molded articles with complicated shapes.
In addition, solid phase polymerization methods are disclosed in Japanese Unexamined Patent Publication (Kokai) Nos. 46398/1972, 84710/1973, 167115/1972, 2549/1974
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