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Solid-state ((2)H, (23)Na, (27)Al) NQR (nuclear quadrupole resonance) spectra of (23)Na- and (27)Al-containing catalysts of the synthesis of tert-butanol or (23)Na- or (27)Al-containing support materials were compared to their solution-state (2)H-NQR spectra. This comparison includes spectra of various catalysts obtained using a combination of support materials and additives such as K(3)PO(4), Cs(2)CO(3), Zr(4)O(7) and Cr(3)O(7). The resolved (23)Na and (27)Al NQR lines agree well with the resolution of experimental (23)Na- or (27)Al-NQR spectra taken in solution. In both solid and solution NQR experiments, hyperfine interactions of (23)Na and (27)Al with (29)Si and (13)C atoms are clearly resolved due to shifts and broadenings of their NQR lines and high degree of order in the solid. For example, in the case of (23)Na in the catalysts the hyperfine interaction of (23)Na with (29)Si atoms is clearly resolved compared to that of (29)Si in solution. However, in the case of (27)Al in Cs(2)CO(3) and Zr(4)O(7) the isotropic hyperfine interaction of (27)Al with (29)Si is not resolved. The resolution and width of the NQR lines depend on the type of shift/broadening involved in the NQR spectroscopy.
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